TY - JOUR
T1 - EFFECTS OF MICROCRYSTALLINE CELLULOSE ON SOME PERFORMANCE PROPERTIES OF CHITOSAN AEROGELS
AU - Ozen, Ertan
AU - Yildirim, Nadir
AU - Dalkilic, Berk
AU - Ergun, Mehmet E.
N1 - Publisher Copyright:
© 2021
PY - 2021
Y1 - 2021
N2 - The aim of this research was to investigate the effect of the microcrystalline cellulose reinforcement on some physical, mechanical, thermal, and morphological properties of the chitosan aerogels. The bio-based chitosan aerogels were produced using chitosan as a matrix and the microcrystalline cellulose as a reinforce material through the freeze-drying method. The aerogel suspensions were prepared in five different ratios to investigate the effect of microcrystalline cellulose content. The density, porosity, thermogravimetric analysis, and compressive resistance tests were conducted according to relevant standards. Morphological properties were investigated using a scanning electron microscope. The introduction of microcrystalline cellulose significantly improved the compressive resistance, thermal properties (Tonset and T%50) of the chitosan aerogels. The optimum performance properties determined as 0,12 MPa for compressive resistance, 0,27 MPa for compressive modulus, 292,45 °C for Tonset and 365 °C for T%50. According to scanning electron microscope images, aerogels showed microporous structure as expected. As a result, the bio-based chitosan aerogels reinforced with microcrystalline cellulose were successfully manufactured. The mechanical and thermal properties including compressive resistance, compressive modulus, Tonset and T%50 of chitosanmicrocrystalline cellulose aerogels found promising.
AB - The aim of this research was to investigate the effect of the microcrystalline cellulose reinforcement on some physical, mechanical, thermal, and morphological properties of the chitosan aerogels. The bio-based chitosan aerogels were produced using chitosan as a matrix and the microcrystalline cellulose as a reinforce material through the freeze-drying method. The aerogel suspensions were prepared in five different ratios to investigate the effect of microcrystalline cellulose content. The density, porosity, thermogravimetric analysis, and compressive resistance tests were conducted according to relevant standards. Morphological properties were investigated using a scanning electron microscope. The introduction of microcrystalline cellulose significantly improved the compressive resistance, thermal properties (Tonset and T%50) of the chitosan aerogels. The optimum performance properties determined as 0,12 MPa for compressive resistance, 0,27 MPa for compressive modulus, 292,45 °C for Tonset and 365 °C for T%50. According to scanning electron microscope images, aerogels showed microporous structure as expected. As a result, the bio-based chitosan aerogels reinforced with microcrystalline cellulose were successfully manufactured. The mechanical and thermal properties including compressive resistance, compressive modulus, Tonset and T%50 of chitosanmicrocrystalline cellulose aerogels found promising.
KW - Aerogels
KW - bio-based
KW - chitosan
KW - compressive resistance
KW - microcrystalline cellulose
KW - scanning electron microscope
KW - thermogravimetric analysis
UR - http://www.scopus.com/inward/record.url?scp=85104737351&partnerID=8YFLogxK
U2 - 10.4067/S0718-221X2021000100426
DO - 10.4067/S0718-221X2021000100426
M3 - Article
AN - SCOPUS:85104737351
SN - 0717-3644
VL - 23
SP - 1
EP - 10
JO - Maderas: Ciencia y Tecnologia
JF - Maderas: Ciencia y Tecnologia
ER -